Unraveling the Cracking Mechanisms of Air Plasma-Sprayed Thermal Barrier Coatings: An In-Situ SEM Investigation

Mohamed Amer, Nicholas Curry, Muhammad Arshad, Qamar Hayat, Vit Janik, Jon Nottingham, Mingwen Bai

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Abstract

In this research work, real-time three-point bending coupled with the scanning electron microscopy (SEM) technique were used to study the crack formation and growth of air plasma spraying (APS) thermal barrier coatings (TBCs). The acquired micrographs were then used to study the strain fields in the vicinity of the cracking region using digital image correlation (DIC) analysis. Fractography analysis for the fractured regions of the APS coatings was also discussed. Based on real-time observation, it was found that roughness of the coatings’ free surface (e.g., valleys) can promote the initiation of cracks since it acts as stress concentration points. Pores and splats features of the coating microstructure contribute to crack branching and crack path deflection, respectively. The former phenomenon (i.e., crack branching) negatively affects the lifetime of the TBC system as it results in an increased fracture area, while the latter can improve the fracture toughness of the coatings and its durability through improving the coating’s ability to dissipate the energy required for crack propagation.
Original languageEnglish
Article number1493
Number of pages24
JournalCoatings
Volume13
Issue number9
Early online date24 Aug 2023
DOIs
Publication statusE-pub ahead of print - 24 Aug 2023

Bibliographical note

© 2023 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https:// creativecommons.org/licenses/by/ 4.0/).

Funder

This research received no funding.

Keywords

  • real-time testing
  • three-point bending (3PB)
  • digital image correlation (DIC)
  • thermal barrier coatings (TBCs)
  • fracture analysis
  • air plasma spray (APS)

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