The Use of Ozone Ashing and Ultrasonic Disintegration as a Sample Preparation Technique for the Determination of Metals in Plant Sections By Slurry Atomisation AAS

Alan Newman; Mark Bateman; Steve Smith; Anne Miller

doi:10.13140/2.1.4962.2086

The Use of Ozone Ashing and Ultrasonic Disintegration as a Sample Preparation Technique for the Determination of Metals in Plant Sections By Slurry Atomisation AAS

Alan Newman, Mark Bateman, Steve Smith, Anne Miller

Oxford Brookes University

Research output: Contribution to conference › Poster › peer-review

Abstract

Ashing at 60-80⁰C in an Ozone atmosphere followed by disruption by ultrasound has been successfully used to prepare plant samples for slurry ETA-AAS . Although the sample preparation time is as long as 5 days the system needs no operator input and for plant microanalysis the system offers significant opportunities. The low temperature ashing prevents loss of volatile analytes. The system currently in use is a set of laboratory built glass chambers each capable of holding 3 samples. The heating has been carried out in a, modified, redundant GC oven.

Original language	English
DOIs	https://doi.org/10.13140/2.1.4962.2086
Publication status	Published - 1996
Event	8th Biennial National Atomic Spectroscopy Symposium - Norwich, United Kingdom Duration: 17 Jul 1996 → 19 Jul 1996 Conference number: 8

Conference

Conference	8th Biennial National Atomic Spectroscopy Symposium
Abbreviated title	BNASS
Country/Territory	United Kingdom
City	Norwich
Period	17/07/96 → 19/07/96

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10.13140/2.1.4962.2086

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The Use of Ozone Ashing and Ultrasonic Disintegration as a Sample Preparation Technique for the Determination of Metals in Plant Sections By Slurry Atomisation AAS. / Newman, Alan; Bateman, Mark; Smith, Steve et al.
1996. Poster session presented at 8th Biennial National Atomic Spectroscopy Symposium, Norwich, United Kingdom.

Research output: Contribution to conference › Poster › peer-review

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title = "The Use of Ozone Ashing and Ultrasonic Disintegration as a Sample Preparation Technique for the Determination of Metals in Plant Sections By Slurry Atomisation AAS",

abstract = "Ashing at 60-80⁰C in an Ozone atmosphere followed by disruption by ultrasound has been successfully used to prepare plant samples for slurry ETA-AAS . Although the sample preparation time is as long as 5 days the system needs no operator input and for plant microanalysis the system offers significant opportunities. The low temperature ashing prevents loss of volatile analytes. The system currently in use is a set of laboratory built glass chambers each capable of holding 3 samples. The heating has been carried out in a, modified, redundant GC oven.",

author = "Alan Newman and Mark Bateman and Steve Smith and Anne Miller",

year = "1996",

doi = "10.13140/2.1.4962.2086",

language = "English",

note = "8th Biennial National Atomic Spectroscopy Symposium, BNASS ; Conference date: 17-07-1996 Through 19-07-1996",

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AU - Newman, Alan

AU - Bateman, Mark

AU - Smith, Steve

AU - Miller, Anne

N1 - Conference code: 8

PY - 1996

Y1 - 1996

N2 - Ashing at 60-80⁰C in an Ozone atmosphere followed by disruption by ultrasound has been successfully used to prepare plant samples for slurry ETA-AAS . Although the sample preparation time is as long as 5 days the system needs no operator input and for plant microanalysis the system offers significant opportunities. The low temperature ashing prevents loss of volatile analytes. The system currently in use is a set of laboratory built glass chambers each capable of holding 3 samples. The heating has been carried out in a, modified, redundant GC oven.

AB - Ashing at 60-80⁰C in an Ozone atmosphere followed by disruption by ultrasound has been successfully used to prepare plant samples for slurry ETA-AAS . Although the sample preparation time is as long as 5 days the system needs no operator input and for plant microanalysis the system offers significant opportunities. The low temperature ashing prevents loss of volatile analytes. The system currently in use is a set of laboratory built glass chambers each capable of holding 3 samples. The heating has been carried out in a, modified, redundant GC oven.

U2 - 10.13140/2.1.4962.2086

DO - 10.13140/2.1.4962.2086

M3 - Poster

T2 - 8th Biennial National Atomic Spectroscopy Symposium

Y2 - 17 July 1996 through 19 July 1996

ER -

The Use of Ozone Ashing and Ultrasonic Disintegration as a Sample Preparation Technique for the Determination of Metals in Plant Sections By Slurry Atomisation AAS

Abstract

Conference

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