The configuration and conformation of the tricyclo[4.4.1.12,5]dodecan‐11‐ols determined by 1H NMR spectroscopy using the shift reagent Eu(fod)3

Timothy J. Mason

doi:10.1002/mrc.1270150324

The configuration and conformation of the tricyclo[4.4.1.1^2,5]dodecan‐11‐ols determined by ¹H NMR spectroscopy using the shift reagent Eu(fod)₃

Timothy J. Mason

University of Warwick

Research output: Contribution to journal › Comment/debate › peer-review

1 Citation (Scopus)

Abstract

The isomeric tricyclo[4.4.1.1^2,5]dodecan‐11‐ols have been synthesized from the (6+4) cycloaddition product of tropone with cyclopentadiene. The configuration and conformation of each isomer was determined from the proton shift gradients induced in the olefinic proton signals in the ¹H NMR spectra of intermediate compounds by Eu(fod)₃.

Original language	English
Pages (from-to)	321-323
Number of pages	3
Journal	Organic Magnetic Resonance
Volume	15
Issue number	3
DOIs	https://doi.org/10.1002/mrc.1270150324
Publication status	Published - Mar 1981
Externally published	Yes

ASJC Scopus subject areas

General Chemistry
General Materials Science

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10.1002/mrc.1270150324

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title = "The configuration and conformation of the tricyclo[4.4.1.12,5]dodecan‐11‐ols determined by 1H NMR spectroscopy using the shift reagent Eu(fod)3",

abstract = "The isomeric tricyclo[4.4.1.12,5]dodecan‐11‐ols have been synthesized from the (6+4) cycloaddition product of tropone with cyclopentadiene. The configuration and conformation of each isomer was determined from the proton shift gradients induced in the olefinic proton signals in the 1H NMR spectra of intermediate compounds by Eu(fod)3.",

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Y1 - 1981/3

N2 - The isomeric tricyclo[4.4.1.12,5]dodecan‐11‐ols have been synthesized from the (6+4) cycloaddition product of tropone with cyclopentadiene. The configuration and conformation of each isomer was determined from the proton shift gradients induced in the olefinic proton signals in the 1H NMR spectra of intermediate compounds by Eu(fod)3.

AB - The isomeric tricyclo[4.4.1.12,5]dodecan‐11‐ols have been synthesized from the (6+4) cycloaddition product of tropone with cyclopentadiene. The configuration and conformation of each isomer was determined from the proton shift gradients induced in the olefinic proton signals in the 1H NMR spectra of intermediate compounds by Eu(fod)3.

UR - https://www.scopus.com/pages/publications/84986754024

U2 - 10.1002/mrc.1270150324

DO - 10.1002/mrc.1270150324

M3 - Comment/debate

AN - SCOPUS:84986754024

SN - 0030-4921

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EP - 323

JO - Organic Magnetic Resonance

JF - Organic Magnetic Resonance

IS - 3

ER -

The configuration and conformation of the tricyclo[4.4.1.1^2,5]dodecan‐11‐ols determined by ¹H NMR spectroscopy using the shift reagent Eu(fod)₃

Abstract

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