Synthesis of Faceted Gamma Alumina Nanoparticles from Waste Beverage Aluminium Cans for Potential Catalyst Support Applications

Rozita Yahaya; Ismail Zainol; Anwar Ul-Hamid Abdulhamid; Hasliza Bahruji; Raja Mazuir Raja Ahsan Shah; Muhammad Hafiz Jasinih; Radiah Salleh

Synthesis of Faceted Gamma Alumina Nanoparticles from Waste Beverage Aluminium Cans for Potential Catalyst Support Applications

Rozita Yahaya, Ismail Zainol, Anwar Ul-Hamid Abdulhamid, Hasliza Bahruji, Raja Mazuir Raja Ahsan Shah, Muhammad Hafiz Jasinih, Radiah Salleh

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Abstract

Green synthesis of gamma alumina (γ-Al₂O₃) nanoparticles (NPs) with facetted and cubeoctahedral morphologies was undertaken from waste (beverage aluminium cans) via precipitation technique and calcination at the temperature of 1000 ^oC. The structural properties of γ-Al₂O₃ were determined with a combination of techniques including BET surface area, field emission scanning electron microscopy (FESEM) with energy dispersive x-ray spectroscopy (EDX), transmission electron microscopy (TEM) and x-ray powder diffraction (XRD). XRD analysis confirmed the formation of γ-Al₂O₃ NPs by comparing with the standard of γ-Al₂O₃ structure. The BET surface area measured was 129 m²/g. High-resolution transmission electron microscopy (HRTEM) analysis provided evidence of surface-enhanced contrast in facetted γ-Al₂O₃ NPs structures similar to the commercial γ-Al₂O₃ NPs.

Original language	English
Article number	8
Journal	Malaysian Journal of Microscopy
Volume	17
Issue number	2
Publication status	Published - 20 Dec 2021

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Yahaya, R., Zainol, I., Abdulhamid, A. U.-H., Bahruji, H., Raja Ahsan Shah, R. M., Jasinih, M. H., & Salleh, R. (2021). Synthesis of Faceted Gamma Alumina Nanoparticles from Waste Beverage Aluminium Cans for Potential Catalyst Support Applications. Malaysian Journal of Microscopy , 17(2), Article 8. https://malaysianjournalofmicroscopy.org/ojs/index.php/mjm/article/view/564

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title = "Synthesis of Faceted Gamma Alumina Nanoparticles from Waste Beverage Aluminium Cans for Potential Catalyst Support Applications",

abstract = "Green synthesis of gamma alumina (γ-Al2O3) nanoparticles (NPs) with facetted and cubeoctahedral morphologies was undertaken from waste (beverage aluminium cans) via precipitation technique and calcination at the temperature of 1000 oC. The structural properties of γ-Al2O3 were determined with a combination of techniques including BET surface area, field emission scanning electron microscopy (FESEM) with energy dispersive x-ray spectroscopy (EDX), transmission electron microscopy (TEM) and x-ray powder diffraction (XRD). XRD analysis confirmed the formation of γ-Al2O3 NPs by comparing with the standard of γ-Al2O3 structure. The BET surface area measured was 129 m2/g. High-resolution transmission electron microscopy (HRTEM) analysis provided evidence of surface-enhanced contrast in facetted γ-Al2O3 NPs structures similar to the commercial γ-Al2O3 NPs.",

author = "Rozita Yahaya and Ismail Zainol and Abdulhamid, {Anwar Ul-Hamid} and Hasliza Bahruji and {Raja Ahsan Shah}, {Raja Mazuir} and Jasinih, {Muhammad Hafiz} and Radiah Salleh",

year = "2021",

month = dec,

day = "20",

language = "English",

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journal = "Malaysian Journal of Microscopy ",

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T1 - Synthesis of Faceted Gamma Alumina Nanoparticles from Waste Beverage Aluminium Cans for Potential Catalyst Support Applications

AU - Yahaya, Rozita

AU - Zainol, Ismail

AU - Abdulhamid, Anwar Ul-Hamid

AU - Bahruji, Hasliza

AU - Raja Ahsan Shah, Raja Mazuir

AU - Jasinih, Muhammad Hafiz

AU - Salleh, Radiah

PY - 2021/12/20

Y1 - 2021/12/20

N2 - Green synthesis of gamma alumina (γ-Al2O3) nanoparticles (NPs) with facetted and cubeoctahedral morphologies was undertaken from waste (beverage aluminium cans) via precipitation technique and calcination at the temperature of 1000 oC. The structural properties of γ-Al2O3 were determined with a combination of techniques including BET surface area, field emission scanning electron microscopy (FESEM) with energy dispersive x-ray spectroscopy (EDX), transmission electron microscopy (TEM) and x-ray powder diffraction (XRD). XRD analysis confirmed the formation of γ-Al2O3 NPs by comparing with the standard of γ-Al2O3 structure. The BET surface area measured was 129 m2/g. High-resolution transmission electron microscopy (HRTEM) analysis provided evidence of surface-enhanced contrast in facetted γ-Al2O3 NPs structures similar to the commercial γ-Al2O3 NPs.

AB - Green synthesis of gamma alumina (γ-Al2O3) nanoparticles (NPs) with facetted and cubeoctahedral morphologies was undertaken from waste (beverage aluminium cans) via precipitation technique and calcination at the temperature of 1000 oC. The structural properties of γ-Al2O3 were determined with a combination of techniques including BET surface area, field emission scanning electron microscopy (FESEM) with energy dispersive x-ray spectroscopy (EDX), transmission electron microscopy (TEM) and x-ray powder diffraction (XRD). XRD analysis confirmed the formation of γ-Al2O3 NPs by comparing with the standard of γ-Al2O3 structure. The BET surface area measured was 129 m2/g. High-resolution transmission electron microscopy (HRTEM) analysis provided evidence of surface-enhanced contrast in facetted γ-Al2O3 NPs structures similar to the commercial γ-Al2O3 NPs.

M3 - Article

SN - 1823-7010

VL - 17

JO - Malaysian Journal of Microscopy

JF - Malaysian Journal of Microscopy

IS - 2

M1 - 8

ER -

Synthesis of Faceted Gamma Alumina Nanoparticles from Waste Beverage Aluminium Cans for Potential Catalyst Support Applications

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