In situ TiC reinforced Ti6Al4V matrix composites manufactured via selective laser melting

  • İdris Tuğrul Gülenç
  • , Mingwen Bai
  • , Ria L. Mitchell
  • , Iain Todd
  • , Beverley J. Inkson

Research output: Contribution to journalArticlepeer-review

13 Citations (Scopus)

Abstract

Purpose: Current methods for the preparation of composite powder feedstock for selective laser melting (SLM) rely on costly nanoparticles or yield inconsistent powder morphology. This study aims to develop a cost-effective Ti6Al4V-carbon feedstock, which preserves the parent Ti6Al4V particle’s flowability, and produces in situ TiC-reinforced Ti6Al4V composites with superior traits. Design/methodology/approach: Ti6Al4V particles were directly mixed with graphite flakes in a planetary ball mill. This composite powder feedstock was used to manufacture in situ TiC-Ti6Al4V composites using various energy densities. Relative porosity, microstructure and hardness of the composites were evaluated for different SLM processing parameters. Findings: Homogeneously carbon-coated Ti6Al4V particles were produced by direct mixing. After SLM processing, in situ grown 100–500 nm size TiC nanoparticles were distributed within the α-martensite Ti6Al4V matrix. The formation of TiC particles refines the Ti6Al4V β grain size. Relative density varied between 96.4% and 99.5% depending on the processing parameters. Hatch distance, exposure time and point distance were all effective on relative porosity change, whereas only exposure time and point distance were effective on hardness change. Originality/value: This work introduces a novel, cost-effective powder feedstock preparation method for SLM manufacture of Ti6Al4V-TiC composites. The in situ SLM composites achieved in this study have high relative density values, well-dispersed TiC nanoparticles and increased hardness. In addition, the feedstock preparation method can be readily adapted for various matrix and reinforcement materials in future studies.

Original languageEnglish
Pages (from-to)378-392
Number of pages15
JournalRapid Prototyping Journal
Volume30
Issue number2
Early online date20 Dec 2023
DOIs
Publication statusPublished - 7 Feb 2024

Funding

This work is supported by the Engineering and Physical Sciences Research Council as a part of “Friction: The Tribology Enigma” ( www.friction.org.uk ), a collaborative Programme Grant between the Universities of Leeds and Sheffield (grant number EP/R001766/1), Manufacture using Advanced Powder Processes (MAPP) programme (grant number EP/P006566/1), Henry Royce Institute for Advanced Materials (grant number EP/R00661X/1). The authors acknowledge the support of the Turkish Government for a PhD studentship (İTG), The University of Sheffield Tomography Centre (STC) [EPSRC (EP/T006390/1)] for XRM data collection, Sorby Centre for Electron Microscopy for imaging, Dr Le Ma for EBSD imaging. The data required to reproduce these findings cannot be shared at this time as the data also forms part of an ongoing study.

FundersFunder number
Ankara Yıldırım Beyazıt Üniversitesi
Sea Turtle Conservancy
Turkish Government
University of Sheffield Tomography Centre
Henry Royce InstituteEP/R00661X/1
Universities of Leeds and SheffieldEP/R001766/1, EP/P006566/1
Engineering and Physical Sciences Research CouncilEP/X527257/1, EP/T006390/1

Keywords

  • Selective laser melting
  • TiC
  • Ti6Al4V
  • In Situ
  • TMCs

ASJC Scopus subject areas

  • Mechanical Engineering
  • Industrial and Manufacturing Engineering

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