Enhanced vacuum glazing bonding strength by anodic bonding assisted sealing method

Hong  Li; Peng Chen; Ping  Zhang; Dehua Xiong; Xin Cao; Lifen Shi; Shou Peng; Yueping Fang

doi:10.1111/ijag.13873

Enhanced vacuum glazing bonding strength by anodic bonding assisted sealing method

Hong Li
, Peng Chen
, Ping Zhang
, Dehua Xiong
, Xin Cao
, Lifen Shi
, Shou Peng
, Yueping Fang

Wuhan University of Technology
State Key Laboratory of Advanced Technology for Float Glass

Research output: Contribution to journal › Article › peer-review

5 Citations (Scopus)

216 Downloads (Pure)

Abstract

A novel sealing method of vacuum glazing is introduced in this study. Anodic bonding technology was used to enhance the bonding strength of the sealant of vacuum glazing. Two sheets of plane glass were sealed by V ₂O ₅-P ₂O ₅-TeO ₂ glass powder with low glass transition temperature (339.3℃) using anodic bonding-assisted low-temperature sintering. Through analyzing the results of Shear Strength test, the diagram of microstructures of the sealing bond taken by a micro Super-depth Microscopy, Scanning Electron Microscope (SEM), and Energy Dispersive Spectrometer (EDS), the best bonding treatment schedule was determined for achieving the strongest bond. The experiment results show that anodic bonding has a dramatic influence on bonding performance. When the sealing temperature and bonding time are kept constant, the shear strength of the sample increases by increasing the bonding voltage. With the bonding temperature of 470℃ and the voltage of 600 V, the air tightness of the sealed sample is 3.9 × 10− ⁹ Pa·m ³/s. The improved bonding strength can enhance life-time of vacuum glazing.

Original language	English
Article number	IJAG13873
Pages (from-to)	147-154
Number of pages	8
Journal	International Journal of Applied Glass Science
Volume	11
Issue number	1
Early online date	8 Sept 2019
DOIs	https://doi.org/10.1111/ijag.13873
Publication status	Published - 1 Jan 2020

Bibliographical note

This is the peer reviewed version of the following article: Li, H, Chen, P, Zhang, P, Xiong, D, Cao, X, Shi, L, Peng, S & Fang, Y 2020, 'Enhanced vacuum glazing bonding strength by anodic bonding assisted sealing method', International Journal of Applied Glass Science, vol. 11, no. 1, IJAG13873, pp. 147-154.which has been published in final form at https://ceramics.onlinelibrary.wiley.com/doi/full/10.1111/ijag.13873. This article may be used for non-commercial purposes in accordance with Wiley Terms and Conditions for Self-Archiving.

Funder

This work was supported by the National Natural Science Foundation of China (51772224, 51372179), Hubei Province Foreign Science and Technology Project (2016AHB027), the Open Fund of the State Key Laboratory of Silicate Materials for Architectures of Wuhan University of Technology (No. SYSJJ2019-14), and the program of (CNBM) Bengbu Design & Research Institute for Glass Industry Co., Ltd. (2019KF01).

Funding

Funders	Funder number
Bengbu Design & Research Institute for Glass Industry Co., Ltd.	2019KF01
China National Building Material
Hubei Province Foreign Science and Technology Project	2016AHB027
Wuhan University of Technology	SYSJJ2019-14
National Natural Science Foundation of China	51372179, 51772224

Keywords

V O -P O -TeO
anodic bonding
bonding strength
low-melting glass
vacuum glazing

ASJC Scopus subject areas

General Materials Science

Access to Document

10.1111/ijag.13873

Post-PrintAccepted author manuscript, 745 KBLicence: Unspecified

Cite this

@article{d0b2ac2c14fa41aab93b7b9488a7a546,

title = "Enhanced vacuum glazing bonding strength by anodic bonding assisted sealing method",

abstract = "A novel sealing method of vacuum glazing is introduced in this study. Anodic bonding technology was used to enhance the bonding strength of the sealant of vacuum glazing. Two sheets of plane glass were sealed by V 2O 5-P 2O 5-TeO 2 glass powder with low glass transition temperature (339.3℃) using anodic bonding-assisted low-temperature sintering. Through analyzing the results of Shear Strength test, the diagram of microstructures of the sealing bond taken by a micro Super-depth Microscopy, Scanning Electron Microscope (SEM), and Energy Dispersive Spectrometer (EDS), the best bonding treatment schedule was determined for achieving the strongest bond. The experiment results show that anodic bonding has a dramatic influence on bonding performance. When the sealing temperature and bonding time are kept constant, the shear strength of the sample increases by increasing the bonding voltage. With the bonding temperature of 470℃ and the voltage of 600 V, the air tightness of the sealed sample is 3.9 × 10− 9 Pa·m 3/s. The improved bonding strength can enhance life-time of vacuum glazing. ",

keywords = "V O -P O -TeO, anodic bonding, bonding strength, low-melting glass, vacuum glazing",

author = "Hong Li and Peng Chen and Ping Zhang and Dehua Xiong and Xin Cao and Lifen Shi and Shou Peng and Yueping Fang",

note = "This is the peer reviewed version of the following article: Li, H, Chen, P, Zhang, P, Xiong, D, Cao, X, Shi, L, Peng, S \& Fang, Y 2020, 'Enhanced vacuum glazing bonding strength by anodic bonding assisted sealing method', International Journal of Applied Glass Science, vol. 11, no. 1, IJAG13873, pp. 147-154.which has been published in final form at https://ceramics.onlinelibrary.wiley.com/doi/full/10.1111/ijag.13873. This article may be used for non-commercial purposes in accordance with Wiley Terms and Conditions for Self-Archiving.",

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AU - Li, Hong

AU - Chen, Peng

AU - Zhang, Ping

AU - Xiong, Dehua

AU - Cao, Xin

AU - Shi, Lifen

AU - Peng, Shou

AU - Fang, Yueping

N1 - This is the peer reviewed version of the following article: Li, H, Chen, P, Zhang, P, Xiong, D, Cao, X, Shi, L, Peng, S & Fang, Y 2020, 'Enhanced vacuum glazing bonding strength by anodic bonding assisted sealing method', International Journal of Applied Glass Science, vol. 11, no. 1, IJAG13873, pp. 147-154.which has been published in final form at https://ceramics.onlinelibrary.wiley.com/doi/full/10.1111/ijag.13873. This article may be used for non-commercial purposes in accordance with Wiley Terms and Conditions for Self-Archiving.

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N2 - A novel sealing method of vacuum glazing is introduced in this study. Anodic bonding technology was used to enhance the bonding strength of the sealant of vacuum glazing. Two sheets of plane glass were sealed by V 2O 5-P 2O 5-TeO 2 glass powder with low glass transition temperature (339.3℃) using anodic bonding-assisted low-temperature sintering. Through analyzing the results of Shear Strength test, the diagram of microstructures of the sealing bond taken by a micro Super-depth Microscopy, Scanning Electron Microscope (SEM), and Energy Dispersive Spectrometer (EDS), the best bonding treatment schedule was determined for achieving the strongest bond. The experiment results show that anodic bonding has a dramatic influence on bonding performance. When the sealing temperature and bonding time are kept constant, the shear strength of the sample increases by increasing the bonding voltage. With the bonding temperature of 470℃ and the voltage of 600 V, the air tightness of the sealed sample is 3.9 × 10− 9 Pa·m 3/s. The improved bonding strength can enhance life-time of vacuum glazing.

AB - A novel sealing method of vacuum glazing is introduced in this study. Anodic bonding technology was used to enhance the bonding strength of the sealant of vacuum glazing. Two sheets of plane glass were sealed by V 2O 5-P 2O 5-TeO 2 glass powder with low glass transition temperature (339.3℃) using anodic bonding-assisted low-temperature sintering. Through analyzing the results of Shear Strength test, the diagram of microstructures of the sealing bond taken by a micro Super-depth Microscopy, Scanning Electron Microscope (SEM), and Energy Dispersive Spectrometer (EDS), the best bonding treatment schedule was determined for achieving the strongest bond. The experiment results show that anodic bonding has a dramatic influence on bonding performance. When the sealing temperature and bonding time are kept constant, the shear strength of the sample increases by increasing the bonding voltage. With the bonding temperature of 470℃ and the voltage of 600 V, the air tightness of the sealed sample is 3.9 × 10− 9 Pa·m 3/s. The improved bonding strength can enhance life-time of vacuum glazing.

KW - V O -P O -TeO

KW - anodic bonding

KW - bonding strength

KW - low-melting glass

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Enhanced vacuum glazing bonding strength by anodic bonding assisted sealing method

Abstract

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ASJC Scopus subject areas

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Yueping Fang

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Enhanced vacuum glazing bonding strength by anodic bonding assisted sealing method

Abstract

Bibliographical note

Funder

Funding

Keywords

ASJC Scopus subject areas

Access to Document

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Fingerprint

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Yueping Fang

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