Defining the limits to long-term nano-indentation creep measurement of viscoelastic materials

Xiaodong Hou, Nigel M Jennett

Research output: Contribution to journalArticle

Abstract

An ultra-stable instrumented nano-indentation tester (UNHT, Anton Paar) was used to study extremely long (30000 seconds) indentation creep of polymers. Total drift rate, measured on fused silica and sapphire samples, was less than 0.2 pm/second for up to 10 hours, enabling collection of valid, low-uncertainty, long-term creep data - orders of magnitude longer than previously possible. Fits of the popular N element Kelvin model to indentation creep data gave values of instant elastic modulus E0 and infinite modulus E∞ strongly dependent on the time-span of data fitted. Comparison with the long-term experimental data showed that the model was unable to use short term data to predict creep at the much longer times required by industry. A new analysis method is proposed to obtain a better estimate of the true value of infinite modulus, E∞, which is the simplest indicator of maximum dimensional change of polymeric material components subject to long-term stress.
LanguageEnglish
Pages297-309
Number of pages13
JournalPolymer Testing
Volume70
Early online date26 Jul 2018
DOIs
Publication statusPublished - Sep 2018

Fingerprint

Nanoindentation
Creep
Indentation
Aluminum Oxide
Polymers
Fused silica
Sapphire
Elastic moduli
Industry

Bibliographical note

NOTICE: this is the author’s version of a work that was accepted for publication in Polymer Testing. Changes resulting from the publishing process, such as peer review, editing, corrections, structural formatting, and other quality control mechanisms may not be reflected in this document. Changes may have been made to this work since it was submitted for publication. A definitive version was subsequently published in Polymer Testing, Vol 70, 2018. DOI: 10.1016/j.polymertesting.2018.07.022

© 2017, Elsevier. Licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 4.0 International http://creativecommons.org/licenses/by-nc-nd/4.0/

Keywords

  • indentation
  • long-term creep
  • viscoelastic
  • modulus

ASJC Scopus subject areas

  • Polymers and Plastics
  • Surfaces, Coatings and Films

Cite this

Defining the limits to long-term nano-indentation creep measurement of viscoelastic materials. / Hou, Xiaodong; Jennett, Nigel M.

In: Polymer Testing, Vol. 70, 09.2018, p. 297-309.

Research output: Contribution to journalArticle

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